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OCR A-level Chemistry A (H432) · Module 4: Core organic chemistry
Mini-Lesson

Core Organic Chemistry

Module 4 is where organic chemistry becomes mechanistic. You stop memorising products and start explaining why a particular bond breaks and a particular product dominates.

Three mechanisms carry the module: free-radical substitution, electrophilic addition and nucleophilic substitution — plus alcohols, isomerism, synthesis routes, infrared and mass spectrometry.

Work through each screen, answer the questions as you go (several are full A-level calculations) and collect ⭐ stars. Press Start when you're ready.

4.1.1 Basic concepts

Isomerism — structural and stereo

Structural isomers have the same molecular formula but a different structural formula: chain isomers, positional isomers and functional group isomers.

Stereoisomers have the same structural formula but a different arrangement in space. At this level that means E/Z isomerism about a C=C double bond, which cannot rotate.

  • E/Z requires two different groups on each carbon of the C=C.
  • Z = the higher-priority groups (by Cahn–Ingold–Prelog: highest atomic number) are on the same side. E = on opposite sides.
  • cis/trans is the special case where one of the two groups on each carbon is an H.

Bond fission: homolytic fission gives each atom one electron — two radicals (shown with single-headed 'fish-hook' arrows). Heterolytic fission gives both electrons to one atom — an ion pair (double-headed curly arrows).

Calculate

Your turn — calculation 1

1A compound contains, by mass, 52.2% C, 13.0% H and 34.8% O, and has Mr = 46.0. How many hydrogen atoms are in its molecular formula? (Ar: C = 12.0, H = 1.0, O = 16.0)
H atoms
Hint: Divide each % by its Ar: C 52.2/12.0 = 4.35, H 13.0/1.0 = 13.0, O 34.8/16.0 = 2.175. Divide all by the smallest (2.175).
Method

Ratios: C 4.35/2.175 = 2, H 13.0/2.175 = 5.98 ≈ 6, O 2.175/2.175 = 1 → empirical formula C₂H₆O, which has M = 46.0 — the same as Mr, so the molecular formula is also C₂H₆O, containing 6 hydrogen atoms (ethanol).

4.1.2 Alkanes

Free-radical substitution

Alkanes are saturated and largely unreactive — the C–C and C–H bonds are strong and almost non-polar. With a halogen and UV light they undergo free-radical substitution, in three stages:

  • Initiation — UV light causes homolytic fission: Cl₂ → 2Cl•
  • Propagation (two steps, and radicals are regenerated):
    Cl• + CH₄ → •CH₃ + HCl
    •CH₃ + Cl₂ → CH₃Cl + Cl•
  • Termination — two radicals combine: •CH₃ + Cl• → CH₃Cl (or •CH₃ + •CH₃ → C₂H₆)

The limitation OCR want you to state: free-radical substitution gives a mixture of products. Further substitution gives CH₂Cl₂, CHCl₃ and CCl₄, and termination steps give a range of by-products, so the yield of any one product is poor.

Quick check

Think it through

?In the chlorination of methane, which step is initiation?
4.1.3 Alkenes

Electrophilic addition and Markovnikov

The C=C double bond has a σ bond plus a π bond formed by sideways overlap of p orbitals. The π electrons sit above and below the plane, are exposed and are attracted to electrophiles — electron-pair acceptors.

Electrophilic addition with HBr on propene:

  • The π electrons attack the δ+ H of H–Br; the H–Br bond breaks heterolytically to give Br⁻.
  • A carbocation intermediate forms; Br⁻ then attacks it.

Markovnikov's rule, explained properly: the major product forms via the more stable carbocation. Stability is tertiary > secondary > primary, because alkyl groups are electron-releasing (positive inductive effect) and spread the positive charge. Propene + HBr therefore gives mainly 2-bromopropane (via the secondary carbocation), not 1-bromopropane.

Alkenes also polymerise: n CH₂=CH₂ → –(CH₂–CH₂)–n. Addition polymerisation has 100% atom economy.

Quick check

Think it through

?Propene reacts with HBr. Why is 2-bromopropane the major product?
Calculate

Your turn — calculation 2

20.0500 mol of an alkene reacts completely with bromine, which adds across the C=C in a 1 : 1 ratio. Calculate the mass of Br₂ required. (Ar: Br = 79.9)
g
Hint: M(Br₂) = 2 × 79.9 = 159.8 g mol⁻¹. mass = n × M.
Method

M(Br₂) = 159.8 g mol⁻¹. mass = 0.0500 × 159.8 = 7.99 g.

4.2.1 Alcohols

Oxidation, elimination and esterification

Alcohols hydrogen-bond, so they have far higher boiling points and much greater water solubility than alkanes of similar Mr.

  • Primary alcohol + acidified K₂Cr₂O₇, distilling the product off immediatelyaldehyde. With excess oxidant under refluxcarboxylic acid.
  • Secondary alcohol + acidified K₂Cr₂O₇ under reflux → ketone. It cannot be oxidised further.
  • Tertiary alcoholnot oxidised (there is no H on the carbon bearing the OH). The dichromate stays orange.
  • Dehydration (elimination of water) with hot concentrated H₂SO₄ or H₃PO₄ → an alkene.
  • Esterification with a carboxylic acid and an acid catalyst → an ester + water.

The colour change to quote: acidified dichromate goes orange (Cr₂O₇²⁻) → green (Cr³⁺) when it oxidises an alcohol. No colour change means a tertiary alcohol.

Calculate

Your turn — calculation 3

30.100 mol of ethanol is oxidised under reflux with excess acidified potassium dichromate to give ethanoic acid, CH₃COOH (M = 60.0). The mass of ethanoic acid isolated is 4.20 g. Calculate the percentage yield.
%
Hint: Theoretical mass = 0.100 × 60.0 = 6.00 g. % yield = (4.20 ÷ 6.00) × 100.
Method

Theoretical = 0.100 mol × 60.0 = 6.00 g. % yield = (4.20 ÷ 6.00) × 100 = 70.0%.

Match it

Match the reagents to the product

Tap a set of reagents and conditions on the left, then the product on the right.

Reagents and conditions
Product
4.2.2 Haloalkanes

Nucleophilic substitution and C–X bond enthalpy

The C–X bond is polar (Cδ+–Xδ−), so the carbon is open to attack by a nucleophile — an electron-pair donor with a lone pair.

  • + warm aqueous NaOH/KOH → alcohol (hydrolysis)
  • + ethanolic KCN, reflux → nitrile (this adds a carbon to the chain — vital in synthesis)
  • + excess ethanolic NH₃ in a sealed tube → amine

Rate of hydrolysis is set by the C–X bond enthalpy, not the electronegativity. C–I is the weakest bond (about 228 kJ mol⁻¹) so iodoalkanes hydrolyse fastest; C–F is the strongest (about 467 kJ mol⁻¹) and is essentially inert. A silver-nitrate-in-ethanol test shows this beautifully: the yellow AgI precipitate appears first, the white AgCl last.

Ozone: CFCs undergo homolytic fission in the stratosphere, releasing Cl• radicals which catalyse ozone breakdown: Cl• + O₃ → ClO• + O₂, then ClO• + O → Cl• + O₂. The Cl• is regenerated, so one radical destroys many ozone molecules.

Quick check

Think it through

?Bromoethane, chloroethane and iodoethane are each warmed with aqueous silver nitrate in ethanol. Which forms a precipitate first, and why?
4.2.4 Analytical techniques

Infrared spectroscopy and mass spectrometry

Infrared: bonds absorb IR at frequencies that make them vibrate. Key absorptions to know:

  • O–H (alcohol) — broad, 3200–3600 cm⁻¹
  • O–H (carboxylic acid)very broad, 2500–3300 cm⁻¹
  • C=O (carbonyl) — strong and sharp, 1630–1820 cm⁻¹ (around 1700)
  • N–H (amine) — 3300–3500 cm⁻¹

The fingerprint region (below 1500 cm⁻¹) is unique to each compound and is used for identification by comparison with a database.

Mass spectrometry: the peak at the highest m/z is the molecular ion peak, M⁺, and it gives the Mr directly. Fragment peaks arise when M⁺ breaks up (e.g. loss of CH₃ = 15, loss of OH = 17, loss of C₂H₅ = 29).

Chlorine gives itself away. Because ³⁵Cl and ³⁷Cl exist in a roughly 3 : 1 ratio, a chlorine-containing compound shows an M⁺ and an M+2 peak with a 3 : 1 height ratio.

Calculate

Your turn — calculation 4

4Propan-1-ol is C₃H₈O. At what m/z value does its molecular ion peak, M⁺, appear? (Ar: C = 12, H = 1, O = 16)
m/z
Hint: M⁺ appears at the Mr of the molecule: (3 × 12) + (8 × 1) + 16.
Method

Mr = 36 + 8 + 16 = 60. Loss of a CH₃ group (15) from this would give a fragment at m/z 45.

Quick check

Think it through

?An unknown compound gives a strong sharp IR absorption at 1715 cm⁻¹ and a very broad absorption from 2500 to 3300 cm⁻¹. What is it likely to be?
Sort it

Which mechanism?

Tap a reaction, then tap the mechanism it follows.

☢️ Free-radical substitution

⚡ Electrophilic addition

🎯 Nucleophilic substitution

4.2.3 Organic synthesis

Building a synthetic route

OCR expect you to plan a two-stage route between any functional groups in the module. Learn the map:

  • alkane → haloalkane (Cl₂ or Br₂, UV)
  • alkene → haloalkane (HBr) · alkene → alcohol (steam, H₃PO₄) · alkene → alkane (H₂, Ni)
  • haloalkane → alcohol (aqueous KOH) · haloalkane → alkene (ethanolic KOH, hot) · haloalkane → nitrile (ethanolic KCN)
  • alcohol → aldehyde (dichromate, distil) → carboxylic acid (dichromate, reflux) · alcohol → alkene (conc. H₂SO₄, dehydration)

The exam's favourite trap: the solvent decides the outcome for a haloalkane and KOH. Aqueous → OH⁻ acts as a nucleophile → substitution → alcohol. Hot and ethanolic → OH⁻ acts as a base → elimination → alkene.

Calculate

Your turn — calculation 5

5Ethanol can be made by fermentation: C₆H₁₂O₆ → 2C₂H₅OH + 2CO₂. Calculate the atom economy for making ethanol, to 1 decimal place. (M: C₆H₁₂O₆ = 180.0, C₂H₅OH = 46.0, CO₂ = 44.0)
%
Hint: Desired product mass = 2 × 46.0. Total product mass = 180.0 (mass is conserved).
Method

Atom economy = (2 × 46.0) ÷ 180.0 × 100 = 92.0 ÷ 180.0 × 100 = 51.1%. Almost half the glucose mass ends up as waste CO₂ — which is why the hydration of ethene (100% atom economy) is used industrially.

Quick check

Think it through

?Which reaction has an atom economy of 100%?
Recap

The big ideas to know

Isomerism: structural (chain, position, functional group) and E/Z stereoisomerism about a C=C

Alkanes: free-radical substitution — initiation (UV, homolytic), propagation, termination; gives a mixture

Alkenes: electrophilic addition via a carbocation; the more stable carbocation gives the major product

Alcohols: primary → aldehyde (distil) → acid (reflux); secondary → ketone; tertiary not oxidised

Haloalkanes: nucleophilic substitution; rate follows C–X bond enthalpy — C–I fastest

Solvent decides: aqueous KOH → substitution; hot ethanolic KOH → elimination

Analysis: IR (broad 2500–3300 = COOH; 1700 = C=O) · MS (M⁺ gives Mr; M+2 at 3 : 1 = chlorine)

That is Module 4 — three mechanisms and a synthesis map you can navigate in both directions. Press Finish to see your score.

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